Preparation and Enhanced Properties of Fe3O4 Nanoparticles Reinforced Polyimide Nanocomposites

Daowei Ding; Xingru Yan; Xi Zhang; Qingliang He; Bin Qiu; Dawei Jiang; Huige Wei; Jiang Guo; Ahmad Umar; Luyi Sun; Qiang Wang; Mojammel A Khan; David P Young; Xin Zhang; Brandon Weeks; Thomas C Ho; Zhanhu Guo; Suying Wei

doi:10.1016/j.spmi.2015.03.008

Preparation and Enhanced Properties of Fe3O4 Nanoparticles Reinforced Polyimide Nanocomposites

Daowei Ding, Xingru Yan, Xi Zhang, Qingliang He, Bin Qiu, Dawei Jiang, Huige Wei, Jiang Guo, Ahmad Umar, Luyi Sun, Qiang Wang, Mojammel A Khan, David P Young, Xin Zhang, Brandon Weeks, Thomas C Ho, Zhanhu Guo, Suying Wei

Research output: Contribution to journal › Article

Abstract

Polyimide (PI) nanocomposite reinforced with Fe3O4 nanoparticles (NPs) at various NPs loadings levels of 5.0, 10.0, 15.0, and 20.0 wt% were prepared. The chemical interactions of the Fe3O4 NPs/PI nanocomposites were characterized using Fourier Transform Infrared (FT-IR) spectroscopy. X-ray Diffraction (XRD) results revealed that the addition of NPs had a significant effect on the crystallization of PI. Scanning electron microscope (SEM) and the atomic force microscope (AFM) were used to characterize the dispersion and surface morphology of the Fe3O4 NPs and the PI nanocomposites. The obtained optical band gap of the nanocomposites characterized using Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS) was decreased with increasing the Fe3O4 loading. Differential scanning calorimetry (DSC) results showed a continuous increase of T-g with increasing the Fe3O4 NPs loading. Some differences were observed in the onset decomposition temperature between the pure PI and nanocomp

Original language	English
Pages (from-to)	305-320
Journal	Superlattices and Microstructures
DOIs	https://doi.org/10.1016/j.spmi.2015.03.008
State	Published - Sep 2015

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Ding, D., Yan, X., Zhang, X., He, Q., Qiu, B., Jiang, D., Wei, H., Guo, J., Umar, A., Sun, L., Wang, Q., Khan, M. A., Young, D. P., Zhang, X., Weeks, B., Ho, T. C., Guo, Z., & Wei, S. (2015). Preparation and Enhanced Properties of Fe3O4 Nanoparticles Reinforced Polyimide Nanocomposites. Superlattices and Microstructures, 305-320. https://doi.org/10.1016/j.spmi.2015.03.008

Ding, Daowei ; Yan, Xingru ; Zhang, Xi ; He, Qingliang ; Qiu, Bin ; Jiang, Dawei ; Wei, Huige ; Guo, Jiang ; Umar, Ahmad ; Sun, Luyi ; Wang, Qiang ; Khan, Mojammel A ; Young, David P ; Zhang, Xin ; Weeks, Brandon ; Ho, Thomas C ; Guo, Zhanhu ; Wei, Suying. / Preparation and Enhanced Properties of Fe3O4 Nanoparticles Reinforced Polyimide Nanocomposites. In: Superlattices and Microstructures. 2015 ; pp. 305-320.

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title = "Preparation and Enhanced Properties of Fe3O4 Nanoparticles Reinforced Polyimide Nanocomposites",

abstract = "Polyimide (PI) nanocomposite reinforced with Fe3O4 nanoparticles (NPs) at various NPs loadings levels of 5.0, 10.0, 15.0, and 20.0 wt% were prepared. The chemical interactions of the Fe3O4 NPs/PI nanocomposites were characterized using Fourier Transform Infrared (FT-IR) spectroscopy. X-ray Diffraction (XRD) results revealed that the addition of NPs had a significant effect on the crystallization of PI. Scanning electron microscope (SEM) and the atomic force microscope (AFM) were used to characterize the dispersion and surface morphology of the Fe3O4 NPs and the PI nanocomposites. The obtained optical band gap of the nanocomposites characterized using Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS) was decreased with increasing the Fe3O4 loading. Differential scanning calorimetry (DSC) results showed a continuous increase of T-g with increasing the Fe3O4 NPs loading. Some differences were observed in the onset decomposition temperature between the pure PI and nanocomp",

author = "Daowei Ding and Xingru Yan and Xi Zhang and Qingliang He and Bin Qiu and Dawei Jiang and Huige Wei and Jiang Guo and Ahmad Umar and Luyi Sun and Qiang Wang and Khan, {Mojammel A} and Young, {David P} and Xin Zhang and Brandon Weeks and Ho, {Thomas C} and Zhanhu Guo and Suying Wei",

year = "2015",

month = sep,

doi = "10.1016/j.spmi.2015.03.008",

language = "English",

pages = "305--320",

journal = "Superlattices and Microstructures",

}

Preparation and Enhanced Properties of Fe3O4 Nanoparticles Reinforced Polyimide Nanocomposites. / Ding, Daowei; Yan, Xingru; Zhang, Xi; He, Qingliang; Qiu, Bin; Jiang, Dawei; Wei, Huige; Guo, Jiang; Umar, Ahmad; Sun, Luyi; Wang, Qiang; Khan, Mojammel A; Young, David P; Zhang, Xin; Weeks, Brandon; Ho, Thomas C; Guo, Zhanhu; Wei, Suying.

In: Superlattices and Microstructures, 09.2015, p. 305-320.

Research output: Contribution to journal › Article

TY - JOUR

T1 - Preparation and Enhanced Properties of Fe3O4 Nanoparticles Reinforced Polyimide Nanocomposites

AU - Ding, Daowei

AU - Yan, Xingru

AU - Zhang, Xi

AU - He, Qingliang

AU - Qiu, Bin

AU - Jiang, Dawei

AU - Wei, Huige

AU - Guo, Jiang

AU - Umar, Ahmad

AU - Sun, Luyi

AU - Wang, Qiang

AU - Khan, Mojammel A

AU - Young, David P

AU - Zhang, Xin

AU - Weeks, Brandon

AU - Ho, Thomas C

AU - Guo, Zhanhu

AU - Wei, Suying

PY - 2015/9

Y1 - 2015/9

N2 - Polyimide (PI) nanocomposite reinforced with Fe3O4 nanoparticles (NPs) at various NPs loadings levels of 5.0, 10.0, 15.0, and 20.0 wt% were prepared. The chemical interactions of the Fe3O4 NPs/PI nanocomposites were characterized using Fourier Transform Infrared (FT-IR) spectroscopy. X-ray Diffraction (XRD) results revealed that the addition of NPs had a significant effect on the crystallization of PI. Scanning electron microscope (SEM) and the atomic force microscope (AFM) were used to characterize the dispersion and surface morphology of the Fe3O4 NPs and the PI nanocomposites. The obtained optical band gap of the nanocomposites characterized using Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS) was decreased with increasing the Fe3O4 loading. Differential scanning calorimetry (DSC) results showed a continuous increase of T-g with increasing the Fe3O4 NPs loading. Some differences were observed in the onset decomposition temperature between the pure PI and nanocomp

AB - Polyimide (PI) nanocomposite reinforced with Fe3O4 nanoparticles (NPs) at various NPs loadings levels of 5.0, 10.0, 15.0, and 20.0 wt% were prepared. The chemical interactions of the Fe3O4 NPs/PI nanocomposites were characterized using Fourier Transform Infrared (FT-IR) spectroscopy. X-ray Diffraction (XRD) results revealed that the addition of NPs had a significant effect on the crystallization of PI. Scanning electron microscope (SEM) and the atomic force microscope (AFM) were used to characterize the dispersion and surface morphology of the Fe3O4 NPs and the PI nanocomposites. The obtained optical band gap of the nanocomposites characterized using Ultraviolet-Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS) was decreased with increasing the Fe3O4 loading. Differential scanning calorimetry (DSC) results showed a continuous increase of T-g with increasing the Fe3O4 NPs loading. Some differences were observed in the onset decomposition temperature between the pure PI and nanocomp

U2 - 10.1016/j.spmi.2015.03.008

DO - 10.1016/j.spmi.2015.03.008

M3 - Article

SP - 305

EP - 320

JO - Superlattices and Microstructures

JF - Superlattices and Microstructures

ER -