Perchlorate in Milk

Andrea B. Kirk, Ernest E. Smith, Kang Tian, Todd A. Anderson, Purnendu K. Dasgupta

Research output: Contribution to journalArticle

154 Scopus citations

Abstract

Perchlorate was unambiguously detected by ion chromatography-suppressed conductivity (IC-CD) and/or ion chromatography-electrospray mass spectrometry (IC-MS) in seven of seven supermarket milk samples bought randomly in Lubbock, TX. Quantitation by IC-MS and IC-suppressed conductivity detection in conjunction with a preconcentration-preelution method provided comparable results. With a sample cleanup procedure that involved protein removal by ethanol and sequential passage though activated alumina and C-18 silica, the limit of detection for perchlorate in milk was 0.5 μg/L. The levels found ranged from 1.7 to 6.4 μg/L. An evaporated milk sample contained perchlorate at 1.1 ± 0.6 μg/L level, while we did not find detectable levels in a reconstituted powdered milk sample.

Original languageEnglish
Pages (from-to)4979-4981
Number of pages3
JournalEnvironmental Science and Technology
Volume37
Issue number21
DOIs
StatePublished - Nov 1 2003

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