Community-Derived Standards for LA-ICP-MS U-(Th-)Pb Geochronology – Uncertainty Propagation, Age Interpretation and Data Reporting

Matthew S.A. Horstwood, Jan Košler, George Gehrels, Simon E. Jackson, Noah M. McLean, Chad Paton, Norman J. Pearson, Keith Sircombe, Paul Sylvester, Pieter Vermeesch, James F. Bowring, Daniel J. Condon, Blair Schoene

Research output: Contribution to journalArticle

215 Scopus citations

Abstract

The LA-ICP-MS U-(Th-)Pb geochronology international community has defined new standards for the determination of U-(Th-)Pb ages. A new workflow defines the appropriate propagation of uncertainties for these data, identifying random and systematic components. Only data with uncertainties relating to random error should be used in weighted mean calculations of population ages; uncertainty components for systematic errors are propagated after this stage, preventing their erroneous reduction. Following this improved uncertainty propagation protocol, data can be compared at different uncertainty levels to better resolve age differences. New reference values for commonly used zircon, monazite and titanite reference materials are defined (based on ID-TIMS) after removing corrections for common lead and the effects of excess 230Th. These values more accurately reflect the material sampled during the determination of calibration factors by LA-ICP-MS analysis. Recommendations are made to graphically represent data only with uncertainty ellipses at 2s and to submit or cite validation data with sample data when submitting data for publication. New data-reporting standards are defined to help improve the peer-review process. With these improvements, LA-ICP-MS U-(Th-)Pb data can be considered more robust, accurate, better documented and quantified, directly contributing to their improved scientific interpretation.

Original languageEnglish
Pages (from-to)311-332
Number of pages22
JournalGeostandards and Geoanalytical Research
Volume40
Issue number3
DOIs
StatePublished - Sep 1 2016

Keywords

  • ICP-MS
  • U-(Th-)Pb geochronology
  • data reporting
  • laser ablation
  • uncertainty propagation

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    Horstwood, M. S. A., Košler, J., Gehrels, G., Jackson, S. E., McLean, N. M., Paton, C., Pearson, N. J., Sircombe, K., Sylvester, P., Vermeesch, P., Bowring, J. F., Condon, D. J., & Schoene, B. (2016). Community-Derived Standards for LA-ICP-MS U-(Th-)Pb Geochronology – Uncertainty Propagation, Age Interpretation and Data Reporting. Geostandards and Geoanalytical Research, 40(3), 311-332. https://doi.org/10.1111/j.1751-908X.2016.00379.x